Inorganic Synthesis, Vol. 30 by Donald W. Murphy, Leonard V. Interrante

By Donald W. Murphy, Leonard V. Interrante

The volumes during this carrying on with sequence offer a compilation of present innovations and concepts in inorganic artificial chemistry. contains inorganic polymer syntheses and education of significant inorganic solids, syntheses utilized in the improvement of pharmacologically energetic inorganic compounds, small-molecule coordination complexes, and similar compounds. additionally comprises priceless info on transition organometallic compounds together with species with metal-metal cluster molecules. All syntheses provided the following were proven.

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J. L. Baberio, K. J. Hansen, D. M. Schleich, and M. J. Martin, J . Electrochem. , 134, 580 (1987). 5. A. J. Jacobson, R. R. Chianelli, and M. S. Whittingham, J. Electrochem. , 126, 2277 (1979). 6. R. R. Chianelli, Catal. Rev. Sci. , 26, 361 (1984). 7. T. A. Pecoraro and R. R. Chianelli, J. , 67,430 (1981). 8. S. Gobolos, Q. Wu, F. Delannay, P. Grange, and B. Delmon, Polyhedron, 5, 219 (1986). 9. R. M. A. Leith and J. C. J. M. Terhell, in Preparation and Crystal Growth ofMaterials with Layered Structures, R.

Anal. Calcd. 42. 2. Properties The rare-earth sesquisulfides are reasonably stable when exposed to air at room temperature, although a weak odor of hydrogen sulfide is frequently present. The orthorhombic A structure is found for La, Ce, Pr, Nd, Sm, Gd, Tb, and Dy. The monoclinic D structure is found for Dy, Ho, Er, and Tm (Dy,S, is dimorphic), and the rhombohedra1 E structure is found for Yb and Lu. The B type of "rare-earth sesquisulfide" has been shown to be an oxysulfide,2 and it is not obtained by this synthesis.

Murphy, Leonard V. Interrante Copyright © 1995 by Inorganic Syntheses, Inc. 38 Binary Compounds 9. LITHIUM NITRIDE, Li,N 6Li + N, + 2Li,N Submitted by E. SCHONHERR,* A. KOHLER,* and G. PFROMMER* Checked by Kj. FI. NIELSENt Reprinted from Inorg. '-' Lithium nitride is formed by direct reaction between lithium metal and nitrogen gas. The reaction goes to completion if the temperature of the lithium and the ambient pressure of the nitrogen are sufficiently high. The synthesis of Li,N ("AzLi,") was first described by Ouvrard,8 who passed nitrogen over glowing lithium in an iron boat.

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